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<DIV><FONT face=Arial size=2>Dear Friends,</FONT></DIV>
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<DIV><FONT face=Arial size=2>I've done one reaction making Amine Hydrochloride
thro' reduction of Oxime with Sodium Metal in n-Propanol. After reduction, TLC
shows complete conversion of Oxime to the Amine. Now during this reaction,
Sodium-n-Propoxide is also being generated as by-product. </FONT></DIV>
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<DIV><FONT face=Arial size=2>Then I passed HCl gas (also tried n-Propanol
HCl) in the post reduction mixture so the Amine get converted to its HCl, but
the reaction mixture becomes quite milky & being difficult to
filter.</FONT></DIV>
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<DIV><FONT face=Arial size=2>Can anyone pls suggest me some good procedure that
how I can do the Amine Hydrochloride with more ease after the reduction
?</FONT></DIV>
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<DIV><FONT face=Arial size=2>Thanx in advance,</FONT></DIV>
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<DIV><FONT face=Arial size=2>Kamal Morendha</FONT></DIV>
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